fire assay cupellation furnace

Fire Assay Laboratory Furnace

Fire Assay Cupellation Furnace for Gold and Silver Assay

The CDOCAST fire assay cupellation furnace is designed for the cupellation stage of precious metal assay, where lead and base metals are oxidized and absorbed by cupels while gold and silver remain as a clean assay bead.

Compared with a standard box furnace, this cupellation furnace is built with controlled oxygen supply, high-temperature uniformity, lead oxide fume exhaust and laboratory safety protection for repeatable gold and silver fire assay results.

ModelCDO-CP fire assay cupellation furnace.
TemperatureMaximum operating temperature 1150°C.
Chamber300 × 200 × 200 mm working chamber.
ApplicationGold assay, silver assay and precious metal laboratory testing.
CDOCAST fire assay cupellation furnace for gold silver assay laboratory

Designed for cupellation, not general heat treatment. The furnace helps maintain an oxidizing atmosphere and remove lead oxide fumes during fire assay.

What Is a Fire Assay Cupellation Furnace?

A fire assay cupellation furnace is a high-temperature laboratory furnace used after fusion in the traditional gold and silver fire assay method. The lead button is placed in a porous cupel and heated under an oxidizing atmosphere.

During cupellation, lead and other base metals oxidize into litharge (PbO) and are absorbed by the cupel. Gold and silver remain as a metallic bead for weighing or further chemical separation.

For laboratories, the key point is repeatability. Stable temperature, controlled oxygen flow and reliable exhaust directly affect cupellation speed, bead cleanliness and assay consistency.

Precious Metal Assay Labs

For gold mining laboratories, refineries, jewelry assay labs, universities and research institutes.

Controlled Oxidation

Dual oxygen flowmeters help the operator adjust oxidizing atmosphere during cupellation.

Lead Oxide Exhaust

A top-mounted exhaust chimney helps discharge PbO fumes generated in the cupellation stage.

Repeatable Test Result

PID control, uniform heating and stable chamber insulation support repeatable fire assay work.

Fire Assay Cupellation Working Process

The cupellation furnace is used after sample fusion. It is not used to replace the full fire assay workflow, but it is the key machine for the lead button oxidation stage.

1Fusion stageThe sample is fused with flux to form a lead button that collects gold and silver.
2Place in cupelThe lead button is placed into a porous cupel suitable for the sample size and assay method.
3CupellationThe furnace heats the cupel under controlled oxidizing atmosphere at high temperature.
4Precious metal beadLead oxide is absorbed by the cupel, leaving a clean gold-silver bead for final analysis.

Machine Details for Cupellation Operation

Control System and Heating Performance

The CDO-CP cupellation furnace uses an intelligent PID programmable controller with up to 30 heating segments. This helps laboratories create repeatable heating curves for gold assay and silver assay work.

U-shaped silicon carbide heating rods are installed on both sides of the chamber for fast heating, temperature uniformity and easier maintenance. The chamber uses vacuum-formed high-purity alumina fiber with multi-layer insulation to reduce heat loss.

  • PID programmable temperature controller with ±1°C control accuracy.
  • Maximum heating rate up to 15°C/min, adjustable according to process need.
  • Temperature uniformity ±5°C within the effective working zone.
  • Type K thermocouple for 0-1200°C measurement range.
touch screen control system for fire assay cupellation furnace PID temperature control

Touch screen control supports programmable heating and easier operation for laboratory technicians.

CDO-CP Fire Assay Cupellation Furnace Specification

ItemSpecificationBuyer Note
ModelCDO-CPStandard laboratory cupellation furnace model.
Furnace TypeFire Assay Cupellation FurnaceDesigned for gold and silver fire assay cupellation stage.
Maximum Operating Temperature1150°CSuitable for common cupellation operation. Higher temperature requires upgraded heating elements.
Temperature Control Range50-1150°CProgrammable temperature control for laboratory workflow.
Chamber Dimensions300 × 200 × 200 mmConfirm cupel size and loading quantity before quotation.
Power SupplyAC 380 VVoltage can be confirmed according to local electrical standard.
Temperature SensorType K thermocouple, 0-1200°CStable temperature feedback for cupellation control.
Temperature Control Accuracy±1°CImportant for repeatable assay conditions.
Temperature Uniformity±5°C within effective working zoneHelps reduce differences between cupel positions.
Heating RateUp to 15°C/min, adjustableSlow heating down to 1°C/h can be programmed when needed.
Heating ElementsU-shaped silicon carbide heating rodsSide-mounted design supports uniform heating and easier replacement.
Chamber MaterialVacuum-formed high-purity alumina fiberLightweight insulation with good thermal cycling resistance.

Why This Furnace Is Different from a Normal Box Furnace

Standard Box Furnace

A normal box furnace is mainly used for heating, sintering, annealing or general laboratory heat treatment. It may not provide controlled oxygen flow or a dedicated exhaust path for lead oxide fumes.

  • General heating chamber.
  • No dedicated dual oxygen flow system.
  • Usually not designed for PbO fume handling.
  • Less suitable for repeatable cupellation work.

Fire Assay Cupellation Furnace

A cupellation furnace is built around the fire assay process. It supports oxidizing atmosphere control, stable chamber temperature, cupel loading and exhaust discharge during lead button oxidation.

  • Controlled air and oxygen supply.
  • Top exhaust chimney for cupellation fumes.
  • Programmable PID heating segments.
  • Designed for gold assay and silver assay laboratories.

Key Features for Precious Metal Assay Laboratories

High-Precision Temperature Control

±1°C control accuracy and up to 30 programmable heating segments support repeatable fire assay cupellation.

Dual Oxygen Flow Control

Independent oxygen flowmeters help adjust the oxidizing atmosphere according to cupellation requirement.

Efficient Exhaust System

The top exhaust chimney helps remove lead oxide fumes and can connect with laboratory fume treatment systems.

SiC Heating Rods

U-shaped silicon carbide heating rods provide fast heating, stable temperature and long service life.

Safe Furnace Housing

Double-layer air-cooled structure helps reduce surface temperature and improve operator safety.

Industrial Construction

CNC machining, phosphating, powder coating and high-temperature baking improve durability and corrosion resistance.

Buyer Checklist Before Quotation

To select a suitable fire assay cupellation furnace, the buyer should confirm the actual laboratory workflow instead of only asking for price.

  • Required chamber dimensions and cupel loading quantity.
  • Operating temperature and heating program requirement.
  • Cupel material, cupel size and sample batch size.
  • Oxygen or air supply condition in the laboratory.
  • Lead oxide fume exhaust and waste gas treatment requirement.
  • Local power supply, voltage and installation environment.

Customization Options

CDOCAST can customize chamber size, voltage, controller configuration, gas flow arrangement and exhaust connection according to the laboratory requirement.

If a higher operating temperature is required, heating elements can be upgraded to silicon carbide or molybdenum disilicide, but the equipment cost will be higher.

For safety, laboratories should plan cupellation furnace exhaust together with local ventilation and environmental treatment requirements.

FAQ About Fire Assay Cupellation Furnace

What is a fire assay cupellation furnace used for?

It is used for the cupellation stage of gold and silver fire assay. The furnace oxidizes lead and base metals under a controlled oxidizing atmosphere, leaving a precious metal bead for weighing or further analysis.

What is the difference between a cupellation furnace and a normal box furnace?

A cupellation furnace has controlled air or oxygen supply and an exhaust system for lead oxide fumes. A normal box furnace is mainly for general heating and usually is not designed specifically for fire assay cupellation.

What temperature does the CDO-CP cupellation furnace operate at?

The standard maximum operating temperature is 1150°C, with a control range from 50°C to 1150°C. If a higher temperature is required, the heating element configuration must be upgraded.

Can CDOCAST supply cupels for fire assay?

Yes. CDOCAST can supply cupels in different materials and sizes according to sample type, cupellation method and laboratory requirement.

Can this furnace test both gold and silver?

Yes. The fire assay cupellation furnace is mainly used for gold and silver assay, especially in gold mining labs, refineries, jewelry assay labs and research laboratories.

What information is needed for quotation?

Please provide chamber size requirement, operating temperature, cupel material and dimensions, gas or oxygen supply condition, waste gas treatment requirement, power supply and expected sample batch size.

What is the warranty?

The standard warranty is one year. Spare parts, heating elements and technical support can be discussed according to the project requirement.

Need a Cupellation Furnace for Your Assay Lab?

Send your cupel size, sample quantity, chamber size requirement, operating temperature and exhaust treatment plan. CDOCAST can recommend a suitable fire assay cupellation furnace configuration for your laboratory.

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